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Identification of Fibers

1. BURN TESTS

Procedure: Cut a small sample of textile fiber and holding it in a tweezer or forceps cautiously ignite with a matchstick or lighter. Observe the sample carefully, because each fiber type will burn in a specific way, producing different colored smake, a particular smell and leaving its own kind of residue. To match your findings with the correct fiber compare with the chart below.

FIBER
Performance at flame
Odor
Residue
 
Approach
to flame
In the
flame
Withdrawn
from flame
   
SILK
Shrinks
away
Burns
slowly
Self
extinguishing
Burning
hair
Brittle, swollen,
black ash
WOOL
Shrinks
away
Burns
slowly
Self
extinguishing
Burning
hair
Brittle, swollen,
black ash
COTTON
No
effect
Burns
readily
Continues
to burn
Burning
paper
Gray
skeletal ash
NYLON
Shrinks
away
Burns slowly
and melts
Often self
extinguishing
Celery
Sometimes
perceptible
Hard light
colored bead
ACRYLIC
Shrinks
away
Burns slowly
and melts
Continues to
burn
and melt
Acrid
Brittle black
bead
POLYPROPYLENE
(OLEFIN)
Shrinks
quickly
Burns
and melts
Burns
and melt
Not defined
Hard, round
bead, maybe
light brown

2. SOLUBILITY OF FIBERS

Some procedures may involve heat, and some some solvents are toxic and corrosive and flammable. Use extreme caution !

 
Acetone 100%
Hydrochloric acid 20%
Sulfuric acid 60%
Sulfuric acid 70%
Chlorine bleach 5%
Formic acid 90%
ACETATE
Soluble
Insoluble
Soluble
Soluble
Insoluble
Soluble
ACRYLIC
Insoluble
Insoluble
Insoluble
Insoluble
depending on type
Insoluble
Insoluble
COTTON
Insoluble
Insoluble
Slightly soluble
Soluble
Insoluble
Insoluble
HAIR
Insoluble
Insoluble
Insoluble
Insoluble
Soluble
Insoluble
HEMP
Insoluble
Insoluble
Slightly soluble
Soluble
Insoluble
Insoluble
LINEN
Insoluble
Insoluble
Slightly soluble
Soluble
Insoluble
Insoluble
MODARYLIC
Soluble or Insoluble
depending on type
Insoluble
Insoluble
Insoluble
Insoluble
Insoluble
NYLON
Insoluble
Soluble
Soluble
Soluble
Insoluble
Soluble
OLEFIN
Insoluble
Insoluble
Insoluble
Insoluble
Insoluble
Insoluble
POLYESTER
Insoluble
Insoluble
Insoluble
Insoluble
Insoluble
Insoluble
RAMIE
Insoluble
Insoluble
Slightly soluble
Soluble
Insoluble
Insoluble
RAYON
Insoluble
Insoluble
Soluble
Soluble
Insoluble
Insoluble
SILK
Insoluble
Partially Soluble
Soluble
Soluble
Soluble
Partially soluble
Wool
Insoluble
Insoluble
Insoluble
Insoluble
Soluble
Insoluble

ADDITIONAL SOLUBILITIES
  • Polypropylene (olefin) soluble in m-xylene and cyclohexanone.
  • Acrylic soluble in dimethyl formamide.
  • Polyester soluble in m-cresol.
  • Nylon 6 is soluble in dimethyl formamide and nylon 66 is not.

3. PHYSICAL PROPERTIES OF FIBERS

Natural Fibers
Density
g/cc
Melting Point
Degree C (Degree F)
CELLULOSE
1.51
None
SILK
1.32-1.34
None
WOOL & OTHER HAIR
1.15-1.30
None
Man-Made Fibers
ACETATE, secondary
1.32
260 (500)
ACETATE, tri.
1.30
288 (550.4)
ACRYLIC
1.12-1.19
None
MODACRYLIC
1.30 or 1.36
188(370.4 not sharp) or 120(248)
NYLON 6
1.12-1.15
213-225(415.4-437)
NYLON 66
1.12-1.15
256-265(492.8-509)
POLYESTER
1.38 or 1.23
250-260(482-500) or 282(539.6 )
POLYPROPYLENE
0.90-0.92
170(338)
RAYON
1.51
None
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